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Briefly, 2 g of PGA (Sigma-Aldrich, 95%) were weighed into a 50 mL volumetric flask and supplemented with 15 mL of 0.02 N methanolic sulfuric acid, with the methanol consisting of either 5% 13 C-labeled methanol (Sigma Aldrich, 99%, 99 atom% 13 C) or unlabeled methanol (Sigma-Aldrich, ≥99.8%)

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